The percentage RSD of the peak area of six replicate injections of S-enantiomer at LOQ concentration was 5.8.The percentage recoveries of S-enantiomer from Lacosamide (LAC) were ranged from 105%-107%.This course material is available from the above address all the time and can be used via web by anyone who wishes to improve the knowledge and skills in analytical method validation (especially when using LC-ESI-MS).Received date: July 12, 2015; Accepted date: July 17, 2015; Published date: July 27, 2015 Citation: Charagondla K (2015) A Validated Chiral Liquid Chromatographic Method for the Enantiomeric Separation of Lacosamide Drug Product and its Dosage Forms. doi:10.4172/2157-7064.1000280 Copyright: © 2015 Charagondla K, et al.
Zaki Pharmaceutical Analytical Chemistry Department Faculty of Pharmacy, Beni-Suef University Alshaheed Shehata Ahmed Hegazy st.
The real-life analysis situations for which there are either examples or self-tests are for example pesticide analyses in fruits and vegetables, perfluororalkyl acids in water, antibiotics in blood serum, glyphosate and AMPA in surface water, etc.
It is important to stress, that for successful validation experience (both in analytical chemistry as such and also specifically in validation) is crucial and this can be acquired only through practice.
The course is largely based on the recently published two-part tutorial review: The course contains lectures, practical exercises and numerous tests for self-testing.
In spite of being introductory, the course intends to offer sufficient knowledge and skills for carrying out validation for most of the common LC-MS analyses in routine laboratory environment.
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